TY  - JOUR
AU  - Vuković, Gorica
AU  - Bursić, Vojislava
AU  - Stojanović, Tijana
AU  - Petrović, Aleksandra
AU  - Gvozdenac, Sonja
AU  - Starović, Mira
AU  - Kuzmanović, Slobodan
AU  - Aleksić, Goran
PY  - 2019
UR  - https://plantarum.izbis.bg.ac.rs/handle/123456789/609
AB  - The undemanding LC-MS/MS method was developed for the synchronized analysis of atropine and scopolamine in maize crop. The dSPE was carried out with 1% acetic acid in acetonitrile/water and a mixture of magnesium sulphate, sodium chloride and sodium citrate. The analytes were separated on a Zorbax XDB C18 column using methanol/water as the mobile phase in gradient mode. The detection was done using a tandem masss spectrometry (MS/MS) in the positive ESI. The tropane alkaloids exhibited excellent linearity in the range of 2-20 µg/kg with the LOQ of 5 µg/kg for maize. The extraction recoveries of atropine and scopolamine were 65.7 and 85.5% with the intraday RSDr 10.25 and 4.29%, respectively. The validated method was appled to real maze samples. One sample contained 18.8 µg/kg of atropine and 6.3 µg/kg of scopolamine.
PB  - Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet
PB  - Novi Sad : Naučni institut za ratarstvo i povrtarstvo
T2  - Savremena poljoprivreda
T1  - LC-MS/MS Determination of Tropane Alkaloids in Maize Crop
EP  - 226
IS  - 3-4
SP  - 221
VL  - 67
DO  - 10.1515/contagri-2018-0032
DO  - 10.1515/contagri-2018-0032
ER  - 

@article{
author = "Vuković, Gorica and Bursić, Vojislava and Stojanović, Tijana and Petrović, Aleksandra and Gvozdenac, Sonja and Starović, Mira and Kuzmanović, Slobodan and Aleksić, Goran",
year = "2019",
abstract = "The undemanding LC-MS/MS method was developed for the synchronized analysis of atropine and scopolamine in maize crop. The dSPE was carried out with 1% acetic acid in acetonitrile/water and a mixture of magnesium sulphate, sodium chloride and sodium citrate. The analytes were separated on a Zorbax XDB C18 column using methanol/water as the mobile phase in gradient mode. The detection was done using a tandem masss spectrometry (MS/MS) in the positive ESI. The tropane alkaloids exhibited excellent linearity in the range of 2-20 µg/kg with the LOQ of 5 µg/kg for maize. The extraction recoveries of atropine and scopolamine were 65.7 and 85.5% with the intraday RSDr 10.25 and 4.29%, respectively. The validated method was appled to real maze samples. One sample contained 18.8 µg/kg of atropine and 6.3 µg/kg of scopolamine.",
publisher = "Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet, Novi Sad : Naučni institut za ratarstvo i povrtarstvo",
journal = "Savremena poljoprivreda",
title = "LC-MS/MS Determination of Tropane Alkaloids in Maize Crop",
pages = "226-221",
number = "3-4",
volume = "67",
doi = "10.1515/contagri-2018-0032, 10.1515/contagri-2018-0032"
}

Vuković, G., Bursić, V., Stojanović, T., Petrović, A., Gvozdenac, S., Starović, M., Kuzmanović, S.,& Aleksić, G.. (2019). LC-MS/MS Determination of Tropane Alkaloids in Maize Crop. in Savremena poljoprivreda
Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet., 67(3-4), 221-226.
https://doi.org/10.1515/contagri-2018-0032

Vuković G, Bursić V, Stojanović T, Petrović A, Gvozdenac S, Starović M, Kuzmanović S, Aleksić G. LC-MS/MS Determination of Tropane Alkaloids in Maize Crop. in Savremena poljoprivreda. 2019;67(3-4):221-226.
doi:10.1515/contagri-2018-0032 .

Vuković, Gorica, Bursić, Vojislava, Stojanović, Tijana, Petrović, Aleksandra, Gvozdenac, Sonja, Starović, Mira, Kuzmanović, Slobodan, Aleksić, Goran, "LC-MS/MS Determination of Tropane Alkaloids in Maize Crop" in Savremena poljoprivreda, 67, no. 3-4 (2019):221-226,
https://doi.org/10.1515/contagri-2018-0032 . .