TY  - JOUR
AU  - Vuković, Gorica
AU  - Đukić, Marina
AU  - Bursić, Vojislava
AU  - Stojanović Petrović, Aleksandra
AU  - Kuzmanović, Slobodan
AU  - Starović, Mira
PY  - 2019
UR  - https://plantarum.izbis.bg.ac.rs/handle/123456789/1007
AB  - The liquid chromatography tandem mass spectrometry (LC-MS/MS) method for the citrinin (CIN) determination in red rice was developed. The mycotoxin was extracted from red rice using anetonitrile/water/acetic acid mixture followed by the clean-up step on Captiva EMR cartridges. The developed method was validated according to the Commission Regulation No. 401/2006/EC. The validation data were evaluated in terms of recoveries, reproducibility, limits of quantification (LOQ), limit of detection (LOD), specificity, linearity and matrix effects for CIN in matrix using 13C20-OTA as an internal standard. The obtained method performance parameters indicate that the method is suitable for the CIN routine analysis.
PB  - University Business Academy, Faculty of Economics and Engineering Management, Novi Sad, Serbia
T2  - Journal of Agronomy, Technology and Engineering Management
T1  - Development and validation of LC-MS/MS method for the citrinin determination in red rice
EP  - 199
IS  - 1
SP  - 192
VL  - 2
ER  - 

@article{
author = "Vuković, Gorica and Đukić, Marina and Bursić, Vojislava and Stojanović Petrović, Aleksandra and Kuzmanović, Slobodan and Starović, Mira",
year = "2019",
abstract = "The liquid chromatography tandem mass spectrometry (LC-MS/MS) method for the citrinin (CIN) determination in red rice was developed. The mycotoxin was extracted from red rice using anetonitrile/water/acetic acid mixture followed by the clean-up step on Captiva EMR cartridges. The developed method was validated according to the Commission Regulation No. 401/2006/EC. The validation data were evaluated in terms of recoveries, reproducibility, limits of quantification (LOQ), limit of detection (LOD), specificity, linearity and matrix effects for CIN in matrix using 13C20-OTA as an internal standard. The obtained method performance parameters indicate that the method is suitable for the CIN routine analysis.",
publisher = "University Business Academy, Faculty of Economics and Engineering Management, Novi Sad, Serbia",
journal = "Journal of Agronomy, Technology and Engineering Management",
title = "Development and validation of LC-MS/MS method for the citrinin determination in red rice",
pages = "199-192",
number = "1",
volume = "2"
}

Vuković, G., Đukić, M., Bursić, V., Stojanović Petrović, A., Kuzmanović, S.,& Starović, M.. (2019). Development and validation of LC-MS/MS method for the citrinin determination in red rice. in Journal of Agronomy, Technology and Engineering Management
University Business Academy, Faculty of Economics and Engineering Management, Novi Sad, Serbia., 2(1), 192-199.

Vuković G, Đukić M, Bursić V, Stojanović Petrović A, Kuzmanović S, Starović M. Development and validation of LC-MS/MS method for the citrinin determination in red rice. in Journal of Agronomy, Technology and Engineering Management. 2019;2(1):192-199..

Vuković, Gorica, Đukić, Marina, Bursić, Vojislava, Stojanović Petrović, Aleksandra, Kuzmanović, Slobodan, Starović, Mira, "Development and validation of LC-MS/MS method for the citrinin determination in red rice" in Journal of Agronomy, Technology and Engineering Management, 2, no. 1 (2019):192-199.

TY  - JOUR
AU  - Vuković, Gorica
AU  - Bursić, Vojislava
AU  - Stojanović, Tijana
AU  - Petrović, Aleksandra
AU  - Gvozdenac, Sonja
AU  - Starović, Mira
AU  - Kuzmanović, Slobodan
AU  - Aleksić, Goran
PY  - 2019
UR  - https://plantarum.izbis.bg.ac.rs/handle/123456789/609
AB  - The undemanding LC-MS/MS method was developed for the synchronized analysis of atropine and scopolamine in maize crop. The dSPE was carried out with 1% acetic acid in acetonitrile/water and a mixture of magnesium sulphate, sodium chloride and sodium citrate. The analytes were separated on a Zorbax XDB C18 column using methanol/water as the mobile phase in gradient mode. The detection was done using a tandem masss spectrometry (MS/MS) in the positive ESI. The tropane alkaloids exhibited excellent linearity in the range of 2-20 µg/kg with the LOQ of 5 µg/kg for maize. The extraction recoveries of atropine and scopolamine were 65.7 and 85.5% with the intraday RSDr 10.25 and 4.29%, respectively. The validated method was appled to real maze samples. One sample contained 18.8 µg/kg of atropine and 6.3 µg/kg of scopolamine.
PB  - Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet
PB  - Novi Sad : Naučni institut za ratarstvo i povrtarstvo
T2  - Savremena poljoprivreda
T1  - LC-MS/MS Determination of Tropane Alkaloids in Maize Crop
EP  - 226
IS  - 3-4
SP  - 221
VL  - 67
DO  - 10.1515/contagri-2018-0032
DO  - 10.1515/contagri-2018-0032
ER  - 

@article{
author = "Vuković, Gorica and Bursić, Vojislava and Stojanović, Tijana and Petrović, Aleksandra and Gvozdenac, Sonja and Starović, Mira and Kuzmanović, Slobodan and Aleksić, Goran",
year = "2019",
abstract = "The undemanding LC-MS/MS method was developed for the synchronized analysis of atropine and scopolamine in maize crop. The dSPE was carried out with 1% acetic acid in acetonitrile/water and a mixture of magnesium sulphate, sodium chloride and sodium citrate. The analytes were separated on a Zorbax XDB C18 column using methanol/water as the mobile phase in gradient mode. The detection was done using a tandem masss spectrometry (MS/MS) in the positive ESI. The tropane alkaloids exhibited excellent linearity in the range of 2-20 µg/kg with the LOQ of 5 µg/kg for maize. The extraction recoveries of atropine and scopolamine were 65.7 and 85.5% with the intraday RSDr 10.25 and 4.29%, respectively. The validated method was appled to real maze samples. One sample contained 18.8 µg/kg of atropine and 6.3 µg/kg of scopolamine.",
publisher = "Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet, Novi Sad : Naučni institut za ratarstvo i povrtarstvo",
journal = "Savremena poljoprivreda",
title = "LC-MS/MS Determination of Tropane Alkaloids in Maize Crop",
pages = "226-221",
number = "3-4",
volume = "67",
doi = "10.1515/contagri-2018-0032, 10.1515/contagri-2018-0032"
}

Vuković, G., Bursić, V., Stojanović, T., Petrović, A., Gvozdenac, S., Starović, M., Kuzmanović, S.,& Aleksić, G.. (2019). LC-MS/MS Determination of Tropane Alkaloids in Maize Crop. in Savremena poljoprivreda
Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet., 67(3-4), 221-226.
https://doi.org/10.1515/contagri-2018-0032

Vuković G, Bursić V, Stojanović T, Petrović A, Gvozdenac S, Starović M, Kuzmanović S, Aleksić G. LC-MS/MS Determination of Tropane Alkaloids in Maize Crop. in Savremena poljoprivreda. 2019;67(3-4):221-226.
doi:10.1515/contagri-2018-0032 .

Vuković, Gorica, Bursić, Vojislava, Stojanović, Tijana, Petrović, Aleksandra, Gvozdenac, Sonja, Starović, Mira, Kuzmanović, Slobodan, Aleksić, Goran, "LC-MS/MS Determination of Tropane Alkaloids in Maize Crop" in Savremena poljoprivreda, 67, no. 3-4 (2019):221-226,
https://doi.org/10.1515/contagri-2018-0032 . .

TY  - JOUR
AU  - Vuković, Gorica
AU  - Bursić, Vojislava
AU  - Aleksic, Goran
AU  - Kuzmanović, Slobodan
AU  - Cara, Magdalena
AU  - Abd El-Wahab, Rania Ahmed
PY  - 2017
UR  - https://plantarum.izbis.bg.ac.rs/handle/123456789/987
AB  - The analysis of citrinin is challenging because it needs to be detected in low concentrations in complex sample matrices. Before citrinin quantification, the data acquisition of LC-MS/MS must be performed, which includes the determination of ion monitoring reaction (SRM), finding fragmentation energies (Frag.) and collision cell energies (CE) for which the response of citrinin will be the highest for the given conditions. The best response of citrinin is obtained for Frag. of 66 V and CE of 17 and 29 V.
PB  - Matica Srpska
T2  - Zbornik Matice srpske za prirodne nauke
T1  - Data acquisition of triple quadrupole LC-MS for the citrinin determination
EP  - 141
SP  - 131
VL  - 133
DO  - 10.2298/ZMSPN1733131V
DO  - 0352-4906
ER  - 

@article{
author = "Vuković, Gorica and Bursić, Vojislava and Aleksic, Goran and Kuzmanović, Slobodan and Cara, Magdalena and Abd El-Wahab, Rania Ahmed",
year = "2017",
abstract = "The analysis of citrinin is challenging because it needs to be detected in low concentrations in complex sample matrices. Before citrinin quantification, the data acquisition of LC-MS/MS must be performed, which includes the determination of ion monitoring reaction (SRM), finding fragmentation energies (Frag.) and collision cell energies (CE) for which the response of citrinin will be the highest for the given conditions. The best response of citrinin is obtained for Frag. of 66 V and CE of 17 and 29 V.",
publisher = "Matica Srpska",
journal = "Zbornik Matice srpske za prirodne nauke",
title = "Data acquisition of triple quadrupole LC-MS for the citrinin determination",
pages = "141-131",
volume = "133",
doi = "10.2298/ZMSPN1733131V, 0352-4906"
}

Vuković, G., Bursić, V., Aleksic, G., Kuzmanović, S., Cara, M.,& Abd El-Wahab, R. A.. (2017). Data acquisition of triple quadrupole LC-MS for the citrinin determination. in Zbornik Matice srpske za prirodne nauke
Matica Srpska., 133, 131-141.
https://doi.org/10.2298/ZMSPN1733131V

Vuković G, Bursić V, Aleksic G, Kuzmanović S, Cara M, Abd El-Wahab RA. Data acquisition of triple quadrupole LC-MS for the citrinin determination. in Zbornik Matice srpske za prirodne nauke. 2017;133:131-141.
doi:10.2298/ZMSPN1733131V .

Vuković, Gorica, Bursić, Vojislava, Aleksic, Goran, Kuzmanović, Slobodan, Cara, Magdalena, Abd El-Wahab, Rania Ahmed, "Data acquisition of triple quadrupole LC-MS for the citrinin determination" in Zbornik Matice srpske za prirodne nauke, 133 (2017):131-141,
https://doi.org/10.2298/ZMSPN1733131V . .