TY  - JOUR
AU  - Vuković, Gorica
AU  - Bursić, Vojislava
AU  - Stojanović, Tijana
AU  - Petrović, Aleksandra
AU  - Gvozdenac, Sonja
AU  - Starović, Mira
AU  - Kuzmanović, Slobodan
AU  - Aleksić, Goran
PY  - 2019
UR  - https://plantarum.izbis.bg.ac.rs/handle/123456789/609
AB  - The undemanding LC-MS/MS method was developed for the synchronized analysis of atropine and scopolamine in maize crop. The dSPE was carried out with 1% acetic acid in acetonitrile/water and a mixture of magnesium sulphate, sodium chloride and sodium citrate. The analytes were separated on a Zorbax XDB C18 column using methanol/water as the mobile phase in gradient mode. The detection was done using a tandem masss spectrometry (MS/MS) in the positive ESI. The tropane alkaloids exhibited excellent linearity in the range of 2-20 µg/kg with the LOQ of 5 µg/kg for maize. The extraction recoveries of atropine and scopolamine were 65.7 and 85.5% with the intraday RSDr 10.25 and 4.29%, respectively. The validated method was appled to real maze samples. One sample contained 18.8 µg/kg of atropine and 6.3 µg/kg of scopolamine.
PB  - Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet
PB  - Novi Sad : Naučni institut za ratarstvo i povrtarstvo
T2  - Savremena poljoprivreda
T1  - LC-MS/MS Determination of Tropane Alkaloids in Maize Crop
EP  - 226
IS  - 3-4
SP  - 221
VL  - 67
DO  - 10.1515/contagri-2018-0032
DO  - 10.1515/contagri-2018-0032
ER  - 

@article{
author = "Vuković, Gorica and Bursić, Vojislava and Stojanović, Tijana and Petrović, Aleksandra and Gvozdenac, Sonja and Starović, Mira and Kuzmanović, Slobodan and Aleksić, Goran",
year = "2019",
abstract = "The undemanding LC-MS/MS method was developed for the synchronized analysis of atropine and scopolamine in maize crop. The dSPE was carried out with 1% acetic acid in acetonitrile/water and a mixture of magnesium sulphate, sodium chloride and sodium citrate. The analytes were separated on a Zorbax XDB C18 column using methanol/water as the mobile phase in gradient mode. The detection was done using a tandem masss spectrometry (MS/MS) in the positive ESI. The tropane alkaloids exhibited excellent linearity in the range of 2-20 µg/kg with the LOQ of 5 µg/kg for maize. The extraction recoveries of atropine and scopolamine were 65.7 and 85.5% with the intraday RSDr 10.25 and 4.29%, respectively. The validated method was appled to real maze samples. One sample contained 18.8 µg/kg of atropine and 6.3 µg/kg of scopolamine.",
publisher = "Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet, Novi Sad : Naučni institut za ratarstvo i povrtarstvo",
journal = "Savremena poljoprivreda",
title = "LC-MS/MS Determination of Tropane Alkaloids in Maize Crop",
pages = "226-221",
number = "3-4",
volume = "67",
doi = "10.1515/contagri-2018-0032, 10.1515/contagri-2018-0032"
}

Vuković, G., Bursić, V., Stojanović, T., Petrović, A., Gvozdenac, S., Starović, M., Kuzmanović, S.,& Aleksić, G.. (2019). LC-MS/MS Determination of Tropane Alkaloids in Maize Crop. in Savremena poljoprivreda
Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet., 67(3-4), 221-226.
https://doi.org/10.1515/contagri-2018-0032

Vuković G, Bursić V, Stojanović T, Petrović A, Gvozdenac S, Starović M, Kuzmanović S, Aleksić G. LC-MS/MS Determination of Tropane Alkaloids in Maize Crop. in Savremena poljoprivreda. 2019;67(3-4):221-226.
doi:10.1515/contagri-2018-0032 .

Vuković, Gorica, Bursić, Vojislava, Stojanović, Tijana, Petrović, Aleksandra, Gvozdenac, Sonja, Starović, Mira, Kuzmanović, Slobodan, Aleksić, Goran, "LC-MS/MS Determination of Tropane Alkaloids in Maize Crop" in Savremena poljoprivreda, 67, no. 3-4 (2019):221-226,
https://doi.org/10.1515/contagri-2018-0032 . .

TY  - JOUR
AU  - Popović, Aleksandra
AU  - Mitrović, Milana
AU  - Petrović, Miloš
AU  - Petrović, Aleksandra
AU  - Bursić, Vojislava
AU  - Marinković, Dušan
AU  - Gvozdenac, Sonja
PY  - 2016
UR  - https://plantarum.izbis.bg.ac.rs/handle/123456789/440
AB  - Based on the number of individuals and percentage of encounters in the studied areas, it is concluded that ground beetles (Coleoptera: Carabidae) stand out in comparison to other beetles, which is proved by the qualitative and quantitative composition of the collected fauna (51 species and 4,420 individuals) in the field of wheat, sugar beet and maize. Starting from the domination of geobiotic insects which spend most of their life in soil and manifest their imaginal activity on the surface of soil, the method of "Barber's traps" was applied. Within this family the dominant and subdominant species during research were Anchomenus dorsalis, Poecilus cupreus, Harpalus rufipes, Calosoma auropunctatum, Harpalu distinguendus and many others. 24 carabids species were determined using the COI mtDNA, i.e. 8 species which don't have reference sequence in the gene bank were determined and this contributes to the global bar-code database. The representatives of ground beetle family are of certain economic significance as well. They can appear as pests; on the other hand, they are known to be very beneficial i.e. as regulators of number of harmful insects as reported in numerous research papers of various authors.
PB  - Ars Docendi, Bucharest
T2  - Romanian Biotechnological Letters
T1  - Molecular Identification of Ground Beetles on Arable Land
EP  - 11364
IS  - 2
SP  - 11357
VL  - 21
ER  - 

@article{
author = "Popović, Aleksandra and Mitrović, Milana and Petrović, Miloš and Petrović, Aleksandra and Bursić, Vojislava and Marinković, Dušan and Gvozdenac, Sonja",
year = "2016",
abstract = "Based on the number of individuals and percentage of encounters in the studied areas, it is concluded that ground beetles (Coleoptera: Carabidae) stand out in comparison to other beetles, which is proved by the qualitative and quantitative composition of the collected fauna (51 species and 4,420 individuals) in the field of wheat, sugar beet and maize. Starting from the domination of geobiotic insects which spend most of their life in soil and manifest their imaginal activity on the surface of soil, the method of "Barber's traps" was applied. Within this family the dominant and subdominant species during research were Anchomenus dorsalis, Poecilus cupreus, Harpalus rufipes, Calosoma auropunctatum, Harpalu distinguendus and many others. 24 carabids species were determined using the COI mtDNA, i.e. 8 species which don't have reference sequence in the gene bank were determined and this contributes to the global bar-code database. The representatives of ground beetle family are of certain economic significance as well. They can appear as pests; on the other hand, they are known to be very beneficial i.e. as regulators of number of harmful insects as reported in numerous research papers of various authors.",
publisher = "Ars Docendi, Bucharest",
journal = "Romanian Biotechnological Letters",
title = "Molecular Identification of Ground Beetles on Arable Land",
pages = "11364-11357",
number = "2",
volume = "21"
}

Popović, A., Mitrović, M., Petrović, M., Petrović, A., Bursić, V., Marinković, D.,& Gvozdenac, S.. (2016). Molecular Identification of Ground Beetles on Arable Land. in Romanian Biotechnological Letters
Ars Docendi, Bucharest., 21(2), 11357-11364.

Popović A, Mitrović M, Petrović M, Petrović A, Bursić V, Marinković D, Gvozdenac S. Molecular Identification of Ground Beetles on Arable Land. in Romanian Biotechnological Letters. 2016;21(2):11357-11364..

Popović, Aleksandra, Mitrović, Milana, Petrović, Miloš, Petrović, Aleksandra, Bursić, Vojislava, Marinković, Dušan, Gvozdenac, Sonja, "Molecular Identification of Ground Beetles on Arable Land" in Romanian Biotechnological Letters, 21, no. 2 (2016):11357-11364.